GCMS analysis results for sample AD31018, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017380–000017404

Folder label: “GCMS X 12/20/01 A 1/8/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) ,**, Data File C:\HPCHEM\1\DATA\JAN0 802\31018.D Vial: 14 - Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 2:49 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.53 152 718027 20.00 ug/1 0.00 10) Naphthalene-d8 15.12 136 2774683 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1367337 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2039952 20.00 ug/1 0.00 38) Chrysene-dl2 32.83 240 1225970 20.00 ug/1 0.00 44) Perylene-dl2 36.90 264 671062 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 29.89 235 108080 4.62 ug/mL -0.18 Spiked Amount 5.000 Recovery = 92.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 192 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 1530 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 19.80 163 361 N.D. 21) 2,6-Dinitrotoluene 20.13 165 357 N.D. 2 2) Acenaphthylene 19.93 152 511 N.D. 23) Acenaphthene 20.49 153 739 N.D. 24) 2,4-Dinitrotoluene 20.84 165 1741 N.D. 25) Diethylphthalate 21.92 149 1556 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.01 166 566 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31018.D GCMS0103.M Wed Jan 09 11:56:43 2002 Page 1

NYC-WTC_000017382

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