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GCMS analysis results for sample AD31018, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017380–000017404

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) $* Data File C:\HPCHEM\1\DATA\JAN0 802\31018.D Vial: 14 • Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS . Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 2:49 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.87 178 1802 N.D.. 34) Anthracene 25.01 178 881 N.D. 35) Di-n-butylphthalate 26.83 149 3963 N.D. 3 6) Fluoranthene 28.51 202 1264 N.D. 3 9) Pyrene 29.16 202 1221 N.D. 40) Butylbenzylphthalate 31.56 149 2547 N.D. 41) Benzo(a)anthracene 32.83 228 4116 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 6067 N.D. 43) Chrysene 32.91 228 1314 N.D. 45) Di-n-Octylphthalate 34.85 149 395 N.D. 4 6) Benzo(b)fluoranthene 35.95 252 1045 N.D. 47) Benzo(k)fluoranthene 35.95 252 595 N.D. 48) Benzo(a)pyrene 36.90 252 3073 N.D. 49) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31018.D GCMS0103.M Wed Jan 09 11:56:46 2002 Page 2

NYC-WTC_000017383

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NYC-WTC_000017383Source: NYC Law Department, mirrored locally

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