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GCMS analysis results for sample AD31074, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) A. ’. ■ Data . File C:\HPCHEM\l\DATA\JAN0802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:16 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 23.91 284 259 N.D. 3 3) Phenanthrene 24.87 178 2047 N.D. 34) Anthracene 25.02 178 1021 N.D. 35) Di-n-butylphthalate 26.83 149 6252 N.D. 36) Fluoranthene 28.50 202 1898 N.D. 3 9) Pyrene 29.16 202 1736 N.D. 40) Butylbenzylphthalate 31.56 149 4259 N.D. 41) Benzo(a)anthracene 32.84 228 4604 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 4386 N.D. 43) Chrysene 32.91 228 1642 N.D. 45) Di-n-Octylphthalate 34.87 149 414 N.D. 4 6) Benzo(b)fluoranthene 35.89 252 1094 N.D. 47) Benzo(k)fluoranthene 35.94 252 479 N.D. 48) Benzo(a)pyrene 36.90 252 3523 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo (g, h, i) perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31074.D GCMS0103.M Wed Jan 09 11:55:40 2002 Page 2

NYC-WTC_000017408

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NYC-WTC_000017408Source: NYC Law Department, mirrored locally

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