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GCMS analysis results for sample AD31074, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) . r" ' . . ; Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D 9 Jan 2002 12:04 am Vial: Operator: 12 209 GALOS Acq On Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:16 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.52 152 842441 20.00 ug/1 0.00 10) Naphthalene-d8 15.12 136 3231484 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1592945 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2353395 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 1419820 20.00 ug/1 0.00 44) Perylene-dl2 36.91 264 816425 20.00 ug/1 0.01

System Monitoring Compounds 37) 2,4-DDD 29.88 235 127824 4.73 ug/mL -0.19 Spiked Amount 5.000 Recovery = 94.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.12 74 314 N.D. 3) bis(2-Chloroethyl)ether 11.00 93 1488 N.D. 4) 1,3-Dichlorobenzene 11.45 146 785 N.D. 5) 1,4-Dichlorobenzene 11.58 146 1177 N.D. 6) 1,2-Dichlorobenzene 12.09 146 905 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. d 9) Hexachloroethane 12.92 117 130 N.D. 11) Nitrobenzene 13.29 77 676 N.D. 12) 1sophorone 13.89 82 1090 N.D. 13) bis(2-Chloroethoxy)methane 14.57 93 810 N.D. 14) 1,2,4-Trichlorobenzene 15.03 180 880 N.D. 15) Naphthalene 15.19 128 4401 N.D. 16) Hexachlorobutadiene 15.74 225 206 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.69 162 1390 N.D. 20) Dimethylphthalate 19.78 163 1523 N.D. 21) 2,6-Dinitrotoluene 20.13 165 444 N.D. 22) Acenaphthylene 19.94 152 1320 N.D. 2 3) Acenaphthene 20.48 153 1622 N.D. 24) 2,4-Dinitrotoluene 20.84 165 814 N.D. 25) Diethylphthalate 21.91 149 2251 N.D. 26) 4-Chlorophenyl-phenylether 22.04 204 219 N.D. 27) Fluorene 22.01 166 1061 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31074.D GCMS0103.M Wed Jan 09 11:55:36 2002 Page 1

NYC-WTC_000017407

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NYC-WTC_000017407Source: NYC Law Department, mirrored locally

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