NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) .
r" ' .
. ; Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D
9 Jan 2002 12:04 am
Vial:
Operator:
12
209 GALOS
Acq On
Sample gems scan 12/20 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 9 10:16 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon Jan 07 10:31:02 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.52 152 842441 20.00 ug/1 0.00
10) Naphthalene-d8 15.12 136 3231484 20.00 ug/1 0.00
17) Acenaphthene-diO 20.39 164 1592945 20.00 ug/1 0.00
29) Phenanthrene-diO 24.81 188 2353395 20.00 ug/1 0.00
38) Chrysene-dl2 32.84 240 1419820 20.00 ug/1 0.00
44) Perylene-dl2 36.91 264 816425 20.00 ug/1 0.01
System Monitoring Compounds
37) 2,4-DDD 29.88 235 127824 4.73 ug/mL -0.19
Spiked Amount 5.000 Recovery = 94.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.12 74 314 N.D.
3) bis(2-Chloroethyl)ether 11.00 93 1488 N.D.
4) 1,3-Dichlorobenzene 11.45 146 785 N.D.
5) 1,4-Dichlorobenzene 11.58 146 1177 N.D.
6) 1,2-Dichlorobenzene 12.09 146 905 N.D.
7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. d
9) Hexachloroethane 12.92 117 130 N.D.
11) Nitrobenzene 13.29 77 676 N.D.
12) 1sophorone 13.89 82 1090 N.D.
13) bis(2-Chloroethoxy)methane 14.57 93 810 N.D.
14) 1,2,4-Trichlorobenzene 15.03 180 880 N.D.
15) Naphthalene 15.19 128 4401 N.D.
16) Hexachlorobutadiene 15.74 225 206 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.69 162 1390 N.D.
20) Dimethylphthalate 19.78 163 1523 N.D.
21) 2,6-Dinitrotoluene 20.13 165 444 N.D.
22) Acenaphthylene 19.94 152 1320 N.D.
2 3) Acenaphthene 20.48 153 1622 N.D.
24) 2,4-Dinitrotoluene 20.84 165 814 N.D.
25) Diethylphthalate 21.91 149 2251 N.D.
26) 4-Chlorophenyl-phenylether 22.04 204 219 N.D.
27) Fluorene 22.01 166 1061 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
31074.D GCMS0103.M Wed Jan 09 11:55:36 2002 Page 1
NYC-WTC_000017407
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