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GCMS analysis log for sample AD31076

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

NYC-WTC_000017514–000017528

Folder label: “GCMS X 12/20/01 A 1/8/02”

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NYC 9/11 Public Portal Document es. . ° Quantitation Report (QT Reviewed) “ Data File : C:\HPCHEM\1\DATA\JAN0802\31076.D Vial: 9 Acq On : 8 Jan 2002 9:09 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc 3 Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:15 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103 Internal Standards R.T. Qlon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.53 152 742895 20.00 ug/1 0.00 10) Naphthalene-ds 15.13 136 2878221 20.00 ug/1 0.00 17) Acenaphthene-d10 20.39 164 1391050 20.00 ug/1 0.00 29) Phenanthrene-d10 24.80 188 2014543 20.00 ug/1 0.00 38) Chrysene-d12 32.84 240 1165047 20.00 ug/1 0.00 44) Perylene-di2 36.90 264 654302 20.00 ug/1 0.00 System Monitoring Compounds 37) 2,4-DDD 29.89 235 102904 4.45 ug/mL -0.18 Spiked Amount 5.000 Recovery = 89.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0) N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 ° N.D. 5) 1,4-Dichlorobenzene 0.00 146 0) N.D. 6) 1,2-Dichlorobenzene 0.00 146 ° N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 ° N.D. 11) Nitrobenzene 0.00 77 ° N.D. 12) Isophorone 13.91 62 209 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 C) N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 1103 N.D. 16) Hexachlorobutadiene 0.00 225 0) N.D. 18) Hexachlorocyclopentadiene 0.00 237 0) N.D. 19) 2-Chloronaphthalene 0.00 162 C) N.D. 20) Dimethylphthalate 19.82 163 207 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 19.94 152 108 N.D. 23) Acenaphthene 20.48 153 346 N.D. 24) 2,4-Dinitrotoluene 20.85 165 611 N.D. 25) Diethylphthalate 21.92 149 1172 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 ° N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 ° N.D. (#) = qualifier out of range (m) = manual integration 31076.D GCMS0103.M Wed Jan 09 11:53:33 2002 Page 1 NYC-WTC_000017516 ‘

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