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GCMS analysis log for sample AD31076

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

NYC-WTC_000017514–000017528

Folder label: “GCMS X 12/20/01 A 1/8/02”

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NYC 9/11 Public Portal Document J Quantitation Report (QT Reviewed) ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31076.D Vial: 9 Acq On : 8 dan 2002 9:09 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:15 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcg Meth : GCMS0103 Compound R.T. QIon Response Conc Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 ° N.D. 33) Phenanthrene 24.87 178 927 N.D. 34) Anthracene 25.01 178 461 N.D. 35) Di-n-butylphthalate 26.83 149 4076 N.D. 36) Fluoranthene 28.52 202 464 N.D. 39) Pyrene 29.17 202 445 N.D. 40) Butylbenzylphthalate 0.00 149 ° N.D. 41) Benzo(a) anthracene 32.84 228 5133 N.D. 42) Bis(2-ethylhexyl)phthalate 33.14 149 1648 N.D. 43) Chrysene 32.84 228 5133 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b) fluoranthene 35.88 252 185 N.D. 47) Benzo (k) fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 36.89 252 2735 N.D. 49) Indeno(1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h) anthracene 0.00 278 ° N.D. 51) Benzo(g,h,i)perylene 0.00 276 ° N.D. (#) = qualifier out of range (m) = manual integration 31076.D GCMS0103.M Wed Jan 09 11:53:37 2002 Page 2 NYC-WTC_000017517

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NYC-WTC_000017517Source: NYC Law Department, mirrored locally

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GCMS analysis log for sample AD31073 · Box DEP Box 16

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

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GCMS analysis log for sample AD31024 · Box DEP Box 16

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

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GCMS scan comments for sample AD31017 · Box DEP Box 16

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Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

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GCMS scan comments for sample AD30605 · Box DEP Box 16

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Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

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