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GCMS scan comments for sample AD31017

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

NYC-WTC_000017364–000017379

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) “ R i ‘ Data File : C:\HPCHEM\1\DATA\JAN0802\31017.D Vial: 13 Acq On : 9 Jan 2002 1:02 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc 3 Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:17 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103 Compound R.T. QIon Response Conc Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0) N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 9 N.D. 33) Phenanthrene 24.87 178 1331 N.D. 34) Anthracene 25.01 178 521 N.D. 35) Di-n-butylphthalate 26.84 149 3308 N.D. 36) Fluoranthene 28.50 202 652 N.D. 39) Pyrene 29.17 202 608 N.D. 40) Butylbenzylphthalate 31.56 149 671 N.D. 41) Benzo (a) anthracene 32.83 228 4414 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 5425 N.D. 43) Chrysene 32.91 228 1022 N.D. 45) Di-n-Octylphthalate 0.00 149 ° N.D. 46) Benzo(b) fluoranthene 35.87 252 206 N.D. 47) Benzo (k) fluoranthene 35.94 252 348 N.D. 48) Benzo(a)pyrene 36.91 252 3250 N.D. 49) Indeno(1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h) anthracene 0.00 278 ° N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D. (#) = qualifier out of range (m) = manual integration 31017.D GCMS0103.M Wed Jan 09 11:56:12 2002 Page 2 NYC-WTC_000017366

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Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

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Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

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GCMS analysis log for sample AD31076 · Box DEP Box 16

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Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

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GCMS blank analysis results · Box DEP Box 16

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Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

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