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GCMS scan comments for sample AD31017

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

NYC-WTC_000017364–000017379

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 2 fae * "bata File : C:\HPCHEM\1\DATA\JAN0802\31017.D Vial: 13 Acq On : 9 dan 2002 1:02 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:17 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103 Internal Standards R.T. Qlon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.52 152 821781 20.00 ug/l 0.00 10) Naphthalene-ds 15.12 136 3183610 20.00 ug/l 0.00 17) Acenaphthene-d10 20.39 164 1558747 20.00 ug/l 0.00 29) Phenanthrene-d10 24.81 188 2338900 20.00 ug/l 0.00 38) Chrysene-d12 32.84 240 1435330 20.00 ug/1 0.00 44) Perylene-d12 36.91 264 825066 20.00 ug/l 0.01 System Monitoring Compounds 37) 2,4-DDD 29.88 235 120726 4.50 ug/mL -0.19 Spiked Amount 5.000 Recovery = 90.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.16 74 107 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.45 146 557 N.D. 5) 1,4-Dichlorobenzene 11.57 146 721 N.D. 6) 1,2-Dichlorobenzene 12.12 146 402 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 ° N.D. 9) Hexachloroethane 12,92 117 117 N.D. 11) Nitrobenzene 0.00 77 0) N.D. 12) Isophorone 13.40 82 115 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0) N.D. 14) 1,2,4-Trichlorobenzene 15.03 180 330 N.D. 15) Naphthalene 15.19 128 1934 N.D. 16) Hexachlorobutadiene 15.73 225 281 N.D. 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 18.69 162 483 N.D. 20) Dimethylphthalate 19.78 163 293 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. a 22) Acenaphthylene 19.95 152 410 N.D. 23) Acenaphthene 20.47 153 882 N.D. 24) 2,4-Dinitrotoluene 20.96 165 198 N.D. 25) Diethylphthalate 21.91 149 1283 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.01 166 323 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 31017.D GCMS0103.M Wed Jan 09 11:56:08 2002 Page 1 NYC-WTC_000017365

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