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GCMS scan comments for sample AD30605

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

NYC-WTC_000017265–000017289

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) ~ Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17 i Acq On : 9 Jan 2002 4:56 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:18 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103 Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.52 152 779642 20.00 ug/1 0.00 10) Naphthalene-ds 15.12 136 3019233 20.00 ug/l 0.00 17)’ Acenaphthene-d10 20.39 164 1484900 20.00 ug/l 0.00 29) Phenanthrene-d10 24.81 188 2196387 20.00 ug/l 0.00 38) Chrysene-di2 32.84 240 1283856 20.00 ug/l 0.00 44) Perylene-di2 36.91 264 716761 20.00 ug/l 0.01 System Monitoring Compounds 37) 2,4-DDD 29.88 235 133611 5.30 ug/ml -0.19 Spiked Amount 5.000 Recovery = 106.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.12 74 263 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0) N.D. 4) 1,3-Dichlorobenzene 0.00 146 0) N.D. 5) 1,4-Dichlorobenzene 0.00 146 0) N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 | 70 0 N.D. 9) Hexachloroethane 0.00. 117 0 N.D. 11) Nitrobenzene 0.00 «77 ° N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.19 128 614 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 0.00 162 0) N.D. 20) Dimethylphthalate 20.12 163 555 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. a 22) Acenaphthylene 20.06 152 393 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.85 165 1925 N.D. 25) Diethylphthalate 21.91 149 2307 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 30605.D GCMSO103.M Tue Jan 15 09:26:47 2002 Page 1 NYC-WTC_000017267

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NYC-WTC_000017267Source: NYC Law Department, mirrored locally

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