NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN0 902\31216.D Vial: 21
Acq On : 10 Jan 2002 10:36 am Operator: 209 GALOS
Sample : gems scan 12/21 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 6 8:43 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Thu Dec 13 14:40:46 2001
Response via : Initial Calibration 2.
DataAcq Meth : GCMS0103 /)
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.52 152 792052 20.00 ug/1 0.00
10) Naphthalene-d8 15.12 136 3096823 20.00 ug/1 0.00
17) Acenaphthene-diO 20.39 164 1555974 20.00 ug/1 0.00
29) Phenanthrene-diO 24.81 188 2217542 20.00 ug/1 0.00
38) Chrysene-dl2 32.83 240 1328036 20.00 ug/1 0.00
44) Perylene-dl2 36.90 264 788277 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 29.88 235 107799 4.24 ug/mL -0.19
Spiked Amount 5.000 Recovery = 84.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.37 74 688 N.D.
3) bis(2-Chloroethyl)ether 10.99 93 861 N.D.
4) 1,3-Dichlorobenzene 11.45 146 551 N.D.
5) 1,4-Dichlorobenzene 11.57 146 973 N.D.
6) 1,2-Dichlorobenzene 12.09 146 481 N.D.
7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 12.93 117 218 N.D.
11) Nitrobenzene 13.27 77 408 N.D.
12) Isophorone 13.90 82 1810 N.D.
13) bis(2-Chloroethoxy)methane 14.56 93 899 N.D.
14) 1,2,4-Trichlorobenzene 15.03 180 509 N.D.
15) Naphthalene 15.18 128 3799 N.D.
16) Hexachlorobutadiene 15.74 225 181 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.68 162 1394 N.D.
20) Dimethylphthalate 19.80 163 2194 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 19.93 152 1895 N.D.
2 3) Acenaphthene 20.48 153 1868 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 21.92 149 2746 N.D.
26) 4-Chlorophenyl-phenylether 22.04 204 736 N.D.
27) Fluorene 22.00 166 1637 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
31216.D GCMS0103.M Wed Feb 06 08:43:53 2002 Page 1
NYC-WTC_000019017
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