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GCMS results for unknowns, sample AD31216, Feb 2002

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GCMS analysis report for sample AD31216 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.

NYC-WTC_000019015–000019024

Folder label: “GCMS X 12/21/01 A 1/10/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\JAN0902\31216.D Vial: 21 Acq On : 10 Jan 2002 10:36 am Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 8:43 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.46 168 538 N.D. 31) 4-Bromophenyl-phenylether 23.50 248 254 N.D. 32) Hexachlorobenzene 23.92 284 726 N.D. 3 3) Phenanthrene 24.87 178 4935 N.D. 34) Anthracene 24.87 178 4935 N.D. 35) Di-n-butylphthalate 26.83 149 21807 N.D. 36) Fluoranthene 28.49 202 3260 N.D. 3 9) Pyrene 29.15 202 3572 N.D. 40) Butylbenzylphthalate 31.34 149 2518 N.D. 41) Benzo(a)anthracene 32.80 228 9897 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 8626 N.D. 43) Chrysene 32.91 228 7735 N.D. 45) Di-n-Octylphthalate 34.88 149 3156 N.D. 46) Benzo(b)fluoranthene 35.89 252 3000 N.D. 47) Benzo(k)fluoranthene 35.89 252 2620 N.D. 4 8) Benzo(a)pyrene 36.74 252 2465 N.D. 49) Indeno(1,2,3-cd)pyrene 40.56 276 641 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 41.63 276 489 N.D.

(#) = qualifier out of range (m) = manual integration 31216.D GCMS0103.M Wed Feb 06 08:43:57 2002 Page 2

NYC-WTC_000019018

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NYC-WTC_000019018Source: NYC Law Department, mirrored locally

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