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GCMS results for unknowns, sample AD31217, Feb 2002

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GCMS analysis report for sample AD31217 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.

NYC-WTC_000019025–000019034

Folder label: “GCMS X 12/21/01 A 1/10/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN0 902\31217.D Vial: 24 Acq On : 10 Jan 2002 1:33 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 8:44 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.87 178 338 N.D. 34) Anthracene 24.87 178 338 N.D. 35) Di-n-butylphthalate 26.83 149 2753 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.84 228 4096 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 1689 N.D. 43) Chrysene 32.91 228 345 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. .46) Benzo (b) fluoranthene 35.97 252 745 N.D. 47) Benzo(k)fluoranthene 35.97 252 871 N.D. 4 8) Benzo(a)pyrene 36.90 252 3756 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31217.D GCMS0103.M Wed Feb 06 08:45:29 2002 Page 2

NYC-WTC_000019028

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NYC-WTC_000019028Source: NYC Law Department, mirrored locally

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