GCMS analysis results for sample AD31345, Feb 2002

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Laboratory report detailing GCMS analysis of sample AD31345 conducted on February 11, 2002.

NYC-WTC_000016970–000016980

Folder label: “GCMS X 12/24/01 A 1/10/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) 2

. , Data File : C:\HPCHEM\1\DATA\JAN0902\31345.D Vial: 11 Acq On : 11 Jan 2002 1:19 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 5 16:38 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.52 152 619489 20.00 ug/1 0.00 10) Naphthalene-d8 15.12 136 2422168 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1238435 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 1711167 20.00 ug/1 0.00 38) Chrysene-dl2 32.83 240 954043 20.00 ug/1 0.00 44) Perylene-dl2 36.90 264 549576 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 29.88 235 79442 4.04 ug/mL -0.19 Spiked Amount 5.000 Recovery = 80.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.12 74 167 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. v 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 697 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.82 165 179 N.D. 25) Diethylphthalate 21.93 149 322 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 31345.D GCMS0103.M Tue Feb 05 16:39:32 2002 Page 1

NYC-WTC_000016972

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