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GCMS calibration table review, Jan-Feb 2002

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Laboratory document detailing GC/MS calibration data for various compounds and method parameters reviewed on January 9, 2002.

NYC-WTC_000016383–000016391

Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\JANO 802\31344.D Vial: 11 Acq On 9 Jan 2002 11:33 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 11:03 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.88 178 556 N.D. 34) Anthracene 24.88 178 556 N.D. 35) Di-n-butylphthalate 26.83 149 4594 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 29.17 202 186 N.D. 40) Butylbenzylphthalate 31.33 149 137 N.D. 41) Benzo(a)anthracene 32.79 228 10075 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 8345 N.D. 43) Chrysene 32.91 228 17164 N.D. 45) Di-n-Octylphthalate 34.88 149 5347 N.D. 46) Benzo(b)fluoranthene 35.94 252 20441 0.28 ug/1 # 92 47) Benzo(k)fluoranthene 35.94 252 20151 0.28 ug/1 # 93 48) Benzo(a)pyrene 36.74 252 5121 N.D. 49) Indeno(l,2,3-cd)pyrene 40.51 276 5911 N.D. 5 0) Dibenz(a,h)anthracene 40.56 278 7543 N.D. 51) Benzo(g,h,i)perylene 41.58 276 8131 N.D.

(#) = qualifier out of range (m) = manual integration 31344.D GCMS0103.M Wed Feb 06 11:04:47 2002 Page 2

NYC-WTC_000016384

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NYC-WTC_000016384Source: NYC Law Department, mirrored locally

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