GCMS calibration table, sample AD31129, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0902\31129A.D Vial: 26 Acq On : 10 Jan 2002 3:31 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

24.95 0.25 ug/1 88403 Phenanthrene-dl0 24.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dl 0- >7 188 C14D10 001719-06-8 86 2 Phenanthrene-d10 188 C14D10 001517-22-2 86 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 53 4 Naphthalene, 2,6-dimethoxy- 188 C12H1202_ 005486-55-5 50 Abundance C Scan 2169 (24.953 mln): 31129A.D (-) m/z 188.10 100.00% 188

5000

80 94 44 55 66 ..132......1581.... Itl ., 253 24.60 24.80 25.00 25.20 Ir X111.. I f'.'i • I 1 ‘ ‘ ‘ I ' i • ■ ■ ' i • ‘ ‘ ■ i m/z 189.10 17.47% miz-> 40__ 60 80 100__ 120 140__ 160 180 200 220 240 Abundance #19957: Anthracene-d10- 188

5000 IS* . T | . iTJ-r.-.-T-J-T 24.60 24.80 25.00 25.20 m/z 184.10 15.65% ................... ...................................................... ............................................................... m/z-> 40 . 60 80__ 100 120 140 160__ 180 200 220 240 Abundance ’ ' i/19e5id Phi apthifono-do 188 ...... {.................... ‘I*/11**14* TTI f 24.60 24.80 25.00 25.20 5000 m/z 94.00 15.32%

RR 80 94 160 00 ! • ‘ i ■ ■ ■ ■ i ■ ■ ■ ' i ■ ■ ■ • i ‘‘ ■ i ■ ■ ' ■ i 1 ■ ‘ ■ i ■ ■ ‘ ■ i

m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #19913: Naphthalene, 1,7-dimethoxy- 9m 173 188 24.60 24.80 25.00 25.20 m/z 8,0.05 15.13% 5000 102 115 145 51 63 75 130 158 1PTTTTTT 1 ■ i ' ■ ■ ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ‘ ‘ i ■ 1 ■ i ■ 1 ■ ■ 1 1 ■ 1 ■ i ■ ‘ ■ i ■ i ' ■ ' ' i • ■ ' 1 i ■ ' ‘ ■ i 1 ' ‘ 1 i ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 24.60 24.80 25.00 25.20

31129A.D GCMS0103.M Wed Feb 06 09:21:37 2002 Page 4

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