Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
NYC-WTC_000018262–000018285Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\DEC3101\30985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.30 6.93 ug/1 2329340 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 N- (Trifluoroacetyl)-N,0,0’,0'’-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 3,4-Di hydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 46 4 Benzoi c acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 Abundance / Scan 1009 (14.305 min): 30985.D (-) m/z 73.0,0 100.00% 73
5000 267 355 • • ■ i • ■ ■ ■ i 1 ■ ■ ’ i ■ • 1 • i ■ • 1 1 i
i 45 14.00 14.20 14.40 14.60 1 miz-> — 50 100 9,125,154 193 233 14 150 200 250 293 ■ i ' 323• 1 i t1 ■ ■ 300 350 400 450 500 550 m/z 267.00 32.95% Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.00 14.20 1440 14.60 ' ‘ m/z 355.0 24.45% .. ...........‘207 . 323 | ' 1 1 1 11 * i ■ 1 1 1 i ‘ i ■ ‘ ' I' m/z-> 50 100 150 200 250 300 ' ' 350 400 450 500 550 Abundance #60162: N-(Trifluoroacety)-N,0.C‘,0"-tetrakis(trimethylsi 73 355 14.00 14.20 14.40 14.60 5000 m/z 356.0 8.53%
45 ____ L 147 193 267 । 538 • 1 ■ i ■ । । • 1 ■ * i ' ‘ 1 1 I 1 * 1 • i ‘ ‘ 1 ■ i ‘ 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868:3.4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- * * I * * * * I * * ‘ r। , i , , , , > , । 73 14.00 14.20 14.40 14.60 m/z 268.00 8.32% 267 5000 179 356 45 147 209 237, 312, i , ............... 11‘ • ■ i • ■ ■ • i • • ' r i ■ • * • i ■ ' ■ ■ i miz-> 50 100 150 200 250 300 350 400 450 500 550 14.00 14.20 14.40 14.60
30985.D GCMS1126.M Wed Jan 23 08:57:09 2002 Page 3
NYC-WTC_000018271
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NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder