Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
NYC-WTC_000018107–000018122Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30695.D Vial: 32 Acq On 1 Jan 2002 6:59 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********** *'* ******************************************************** Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.30 1.55 ug/1 456884 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 46 3 Benzoic cid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 4 N- (Trif uoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 38 Abundance/ Scan 1009 (14.303 min): 30695.D (-) m/z 73.0.0 100.00% 73
5000 267 355 **I***I**1‘+‘-III 45 , 89 108 133 154 177 193 . 223i . 251 , 293 323339 [ 14.00 14.20 14.40 14.60 m/z-> H "i । r saltasjoataternpure Trrss I'm ti. ;t. j 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 m i । .t» । |i » । .-j ।».11 h .»j m/z 267.00 30.53% Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 ’ • I • • 14,00 14,20 14.40 14.60 m/z 355.0 21.42% 191207 251 . 323339 i ■ ‘1 ‘ I" ■ ‘ i TTT * i' ’ * ‘ i *1 i “ ** i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dinydroxybenzyl alcohol,tris(trimethylsily!)- 73
267 14.00 14.20 14.40 14.60 5000 179 m/z 356.0 8.44% 356 45 147 209 237 ′ 312 ‘‘1‘21‘37111931111——0033370n3ttt211 • > j 111111111 11 > > < 11 / rrpTj rp i1i1 i j t i1' i i1 i p i । j । miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-> trimet - 73 355 14.00 14.20 14*40 14.60 m/z 268.00 7.78% 5000
147 267
‘ 47 , 118 2 23 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 1 14.00 14.20 14.40 14.60
30695.D GCMS1126.M Wed Jan 23 08:33:34 2002 Page 3
NYC-WTC_000018116
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NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder