Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
NYC-WTC_000018107–000018122Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30695.D Vial: 32 Acq On 1 Jan 2002 6:59 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************* ******************************************************** Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 1.88 ug/1 555243 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 32 3 1,1,1,5,7/7,7-Heptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 27 4 2H-1,4-Renzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 12 Abundance Scan 1352 (17.452 min): 30695.D (-) m/ z 73.0,0 100.00% 73
5000 341 147 ■ ITT ' 1 • i ■ ■ 45 429 17.20 17.40 17.60 17.80 miz-> mhhm 117 , [ 179.. 207225 251269 295 323 : humnutmoha—aO—8B16uua——aah—GBmn—Bap—BmTg3d2493AA2a28p3 ............. 40 60 80 100120140160180200220240260280300320340360380400420 ........ ’1*4411444*72414 m/z 341.00 2 7.79% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341 i 429 5000 17.20 17.40 17.60 17.80 147 m/z 147.00 13.35% 207 267 117 —[ B3BB878 TTmmpp" 311 [ Bu——01000009013unB Tp m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48317: 4-Amino-5-imidazole carboxamide, tris(trimethyisily 73 T T T T 327 17.20 17.40 17.60 17.80 5000 m/z 342.00 9.62% 237 45
m/z-> 1......... .147 ............................... . 40 60 80 100120140160180200220246260280300320340360380400420 ' Abundance #56714; 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 17.20 17.40 17.60 17.80 m/z 325.00 9.26% 147 5000 267 355 429 45 207 .... ....... ................ 1 ............... Il.............. ................. _ 1111 j 11 • < । > * h ।* 1111 k <* 111 <f1141:111 > > • ।> i > i ]ii nf i n't] i n1111 fn i rpnr|ti 11 pk n p 11 rp 111 p r 11 p ijT T T ' I ' ‘ ‘ ' I ' ' miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420. 17.20 17.40 17.60 17.80
30695.D GCMS1126.M Wed Jan 23 08:33:39 2002 Page 4
NYC-WTC_000018117
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NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder