Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
NYC-WTC_000018287–000018315Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\JAN1 8 02 \ 3 0 9 8 6A. D Vial: 3 Acq On 18 Jan 2002 5:36 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.27 5.93 ug/1 2825360 Naphthalene-d8 15.09
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 1,1,1,5,7<7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 27 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 12 4 4-Amijfo-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 9 Abundance Scan 1332 (17.275 min): 30986A.D (-) m/z 73.0,0 100.00% 73
5000 341 45 [ 147 179 207225 251 281 311 L 397 429 17.00 17.20 17.40 17.60 miz-> +A96..117 TI—pgmpmmp m/z 341.00 40 60 80 100120140160180200220240260280300320340360380400420 27.94% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 ■ ■ i ■ ■ ■ ■ i ■ i ■ ' 17.00 17.20 17.40 17.60 147 m/z 147.00 14.03% 117 | 207 267 311 [ .! I. I. I.. A ,. 1 .i 1.... I. H i 1.1.. |.... (. 1. 111 M 11.»I»[ JI». |. 11.. > 11»i. IJ r... ’ ’I’IUUBUI-1* m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 ^Abundance *58714: 1.1,1.5./.7.7-Heptamethyl-3.3-bis(tnmethylsiloxy)t 73
147 17.00 17.20 17.40 17.60 5000 267 m/z 325.00 9.36% 355 429 45 207
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 17.00 17.20 17.40 17.60 m/z 342.00 9.35% 5000 45 91 I 116 146 Tpmmpp 227 269 TTTTTTTTTTptTTpTTrp^TTpTTTpTTTfrrrrfhT^^ 315 [ _ 0 PPI m/z—> 40 60 80 100120140160180 200 220240 260 280 300 320 340360380400 420 17.00 17.20 17.40 17.60
30986A.D GCMS1126.M Tue Jan 22 10:18:02 2002 Page 9
NYC-WTC_000018303
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
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NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
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NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
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NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
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NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
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