NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30695.D vial: 32
Acq On 1 Jan 2002 6:59 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 5 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
20.28 1.04 ug/1 337096 Acenaphthene-dl0 20.56
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethy1 576 C18H52O7Si7 071579-69-6 38
2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 33
3 Octade'canoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 9
4 Phosphoric acid, 3-(ethoxyimino)-2- 429 C14H36NO6PSi3 055334-96-8 9
Abundance / Scan 1660 (20.280 min): 30695.D (-) m/z 73.0,0 100.00%
73
5000
147 281 . . ....
327
45 20.00 20.20 20.40 20.60
miz-> 50
+ 117
*t* T-Tt
100
-.46383,415.. ...
191 221 249
rih Pi 1trt
150 200 250 300 350 400 450 500 550
m/z 147.00 35.66%
Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
5000
147 20.00 20.20 20.40 20.60
221 281 m/z 281.00 33.46%
327 415 519 561
■ • i • ■ ■ ■ I ' • ■ ■ i • • • • i ■ - TI————m—T
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459; Trisiloxane, 1.1,1 5.5,5-hexamethy-3,3-bis[(trimet
73 147
281 20.00 20.20 20.40 20.60
5000 m/z 326.90 13.81%
1207 249 369
338 i...............
miz-> 50 100 150 200 * 250 300 350 400 450 500 550
Abundance #74127: Octadecanoic acid, 2-[(trimethylsilyl)oxy]-, methyl ■ • i ' 1
73 327 20.00 20.20 20.40 20.60
m/z 282.00 8.65%
5000
371
103
t
t 129 159
"l 7 / । I ■! I | I . -
1 * i
miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20'20 20'40 20.60
30695.D GCMS1126.M Wed Jan 23 08:33:45 2002 Page 5
NYC-WTC_000018118
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