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GCMS analysis log for sample AD30695, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.

NYC-WTC_000018107–000018122

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018118
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30695.D vial: 32 Acq On 1 Jan 2002 6:59 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

20.28 1.04 ug/1 337096 Acenaphthene-dl0 20.56

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamethy1 576 C18H52O7Si7 071579-69-6 38 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 33 3 Octade'canoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 9 4 Phosphoric acid, 3-(ethoxyimino)-2- 429 C14H36NO6PSi3 055334-96-8 9 Abundance / Scan 1660 (20.280 min): 30695.D (-) m/z 73.0,0 100.00% 73

5000 147 281 . . .... 327 45 20.00 20.20 20.40 20.60 miz-> 50 + 117 *t* T-Tt 100 -.46383,415.. ... 191 221 249 rih Pi 1trt 150 200 250 300 350 400 450 500 550 m/z 147.00 35.66% Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 20.00 20.20 20.40 20.60 221 281 m/z 281.00 33.46% 327 415 519 561 ■ • i • ■ ■ ■ I ' • ■ ■ i • • • • i ■ - TI————m—T miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459; Trisiloxane, 1.1,1 5.5,5-hexamethy-3,3-bis[(trimet 73 147 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 13.81%

1207 249 369 338 i............... miz-> 50 100 150 200 * 250 300 350 400 450 500 550 Abundance #74127: Octadecanoic acid, 2-[(trimethylsilyl)oxy]-, methyl ■ • i ' 1 73 327 20.00 20.20 20.40 20.60 m/z 282.00 8.65% 5000 371 103 t t 129 159 "l 7 / । I ■! I | I . - 1 * i miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20'20 20'40 20.60

30695.D GCMS1126.M Wed Jan 23 08:33:45 2002 Page 5

NYC-WTC_000018118

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NYC-WTC_000018118Source: NYC Law Department, mirrored locally

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