Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
NYC-WTC_000018605–000018623Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\DEC3101\30705.D Vial: 46 Acq On 2 Jan 2002 9:30 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 20.28 1.63 ug/1 527618 Acenaphthene-dl0 20.57 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 3-Isopropoxy-1,1,1,7,7,7 -hexamethyl 576 C18H5207Si7 071579-69-6 38 3 Octadecanoic acid, 2-(trimethylsil 386 C22H46O3Si 056196-58-8 9 4 Phosphoric acid, 2-/methoxyimino) -3 415 C13H34NO6PSi3 055319-85-2 9 Abundance Scan/660 (20.281 min): 30705.D (-) m/z 73.00 100.00% 73
5000 147 281 327 ■ 1 i 1 1 TTT’l 1 20.00 20.20 20.40 20.60 : oA 45 -4+ 117 1 F* 191,221 Pit251 191,221251 rnih rr. 300 ‘‘ 350 , 383,415. . m/z 147.00 35.00% miz-> 50 100 150 200 250 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 —------- 5000 20.00 20.20 20.40 20.60 369 m/z 281.0,0 32.69% f 207 249, *. 38 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1.1,1.7,7 7-hexamethyl-3,5,5-tris(trim 73 20.00 20.20 20.40 20.60 5000 m/z 326.90 13.57% 147 221 ■ 281 327 415 I 519 561 Tnnn—nnmTn1/t1’3 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52732: Octadecanoic acid, 2-[(trimethylsilyf)oxy]-, methyl _________ /_________ I I I I 1 1 I I I I J J I i t I I I I I
73 20.00 20.20 20.40 20.60 m/z 282.0.0 9.78% 5000 327
1103129 159 371 T-r-p- i .W । J.. i, * i * ■ * » । ' i * • । । ‘ I ' * * * I ■ "i । ■ । । > • ‘ l ‘ ‘ ‘ ‘ I ‘ ‘ 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30705.D GCMS1126.M Fri Jan 25 11:27:11 2002 Page 4
NYC-WTC_000018615
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NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder