Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
NYC-WTC_000018142–000018154Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\DEC3 10130711.D Vial: 34 Acq On 1 Jan 2002 8:55 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************* * * Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 14.31 0.46 ug/1 143495 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 N- (Trifluoroacetyl)-0,0',0' ’-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 3 Benzoic cid, 2-[ (trimethylsilyl) ox 282 C13H2203Si2 003789-85-3 43 4 Benzeneethanamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 43 Abundance Scan 1009 (14.305 min): 30711.D (-) m/z " 100.00% 73
5000 267 355 T 1 FI7 II I- » J J II t I I't I I p'l 45 108 133154 193 223 323 14.00 14.20 14.40 14.60 — *1′1* ■ ‘i " i 1 ■ • ' i ■ ■ ' • i ■ ■ ■ ■ i 1 ■ m/z 267.00 31.58 mz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 11444414 13778 ■ 1 1 14.00 14.20 14.40 14.60 m/z 355.0 22.70 . , 207 ... 323 , I ' ' i 1 ‘ ‘ ■ i ' ■ • ■ 1 • ■ ■ 1 i • • lt । > i i । । m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-{Trifuoroacetyh-0.0‘,0"-tris(trimethylsilyl)no i 73 355 14.00 14.20 14.40 14.60 5000 m/z 267.9,0 9.06
45 126147 193 265 : 376 481 • ‘ i • 1 T' l ‘ 1 ‘ ‘ I ' ‘ ‘ Lr-T-r-r-]—r-T—r-r-j—r m/z-> 50 100 150 200 250 300 350 11**11* 400 450 Abundance #72301: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsi ■ • i ■ ■ ■ 1 i 1 1 1 > i 1 1 * ' i ' 1 1 1 i 73 14.00 14.20 14.40 14.60 m/z 74.00 8.56 5000 267 45
miz-> .,...35193__ 50 100 ' ' 150 ‘ ’ '260 ' ‘ 250 IIIIIIT ‘ 1 i ‘ 1 ■ 1 i ■ ■ 1 ' i 1 1 1 1 I 1 1 1 1 I 300 350 400 450 14.00 14.20 14.40 14.60
30711.D GCMS1126.M Wed Jan 23 08:39:03 2002 Page 3
NYC-WTC_000018151
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NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018248
Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016783
GCMS analysis of environmental sample AD30118 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049762
GCMS analysis report for sample AD31640 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049734
GCMS analysis report for sample AD31642 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036831
Gas chromatography-mass spectrometry analysis of sample AD29666 identifying unknown compounds and surrogate recovery data (2,4-DDD at 72%), January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder