Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
NYC-WTC_000018142–000018154Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30711.D Vial: 34 Acq On 1 Jan 2002 8:55 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 4-Amino-5-imidazole carboxamid Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 17.45 0.48 ug/1 148451 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 25 2 Cyclohexasilo: ne, dodecamethyl- 444 C12H36O6Si6 000540-97-6 25 3 1,1,1,5,7,77 -Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 9 4 Silane, 2 ,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 7 Abundance Scan 1352 (17.454 min): 30711.D (-) m/z 73.0,0 100.00% 73
5000 341 । « । t“i—»■» । i i 4} r > i । । i i 45 147 429 207 17.20 17.40 17.60 17.80 .................. ...... 117 251 295 ............................................................................................................... m/z 341.00 27.21% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 ( f l ) j i I i > ) y [ . I ] I T _ 327 5000 237 17.20 17.40 17.60 17.80 45 m/z 147.00 13.77% 147 | 172 212 L U“I——B9BO0108119378" ] ■। ।. ■.. ।.. >. ।.... (. j.. pYrrpTTTpTTTpTTTp- "EEE"TTIT I UII‘ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxare, dodecamethyl- 73 341
429 17.20 17.40 17.60 17.80 5000 m/z 325.00 10.68% 147 117 267 311 , 207 vrTTTrrrrrrrm-rr Ipmeamnap—anp—nar TTpg Th m/z-> Abundance 40 60 80 100120140160180200220240260280300320340360380400420 #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 T 4 T 17.20 17.40 17.60 17.80 m/z 342.00 8.74% 147 5000 267 355 429 45 207
TT TIT TT |Hi.|.lhpT»I|TTD[ I I j *» »( | i »..jir » »।I i i t| I ‘•1**‘1*‘‘‘I***‘I** m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30711.D GCMS1126.M Wed Jan 23 08:39:08 2002 Page 4
NYC-WTC_000018152
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NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018248
Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016783
GCMS analysis of environmental sample AD30118 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049762
GCMS analysis report for sample AD31640 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049734
GCMS analysis report for sample AD31642 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036831
Gas chromatography-mass spectrometry analysis of sample AD29666 identifying unknown compounds and surrogate recovery data (2,4-DDD at 72%), January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder