GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
NYC-WTC_000036815–000036830Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\29667.D Vial: 56 Acq On 2 Jan 2002 8:14 pm Operator: 209 GALOS Sample gems scan 12/7 . Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 6 4-Amino-5-imidazole carboxamid Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
17.45 0.70 ug/1 351731 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 32 2 1,1,1,5,7,7Z7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 3 2H-1,4-B zodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 12 Abundance Scan 1352 (17.454 min): 29667.D() m/ z 73.0,0 100.00% 73
5000 - 341 ----- 147 45 429 17.20 17.40 17.60 17.80 m/z-> mk , 117 [ 179 207 251 281 311 L ( TTE"IETTuuor mTTT m/z 341.00 26.43% 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380400420 Abundance #48317: 4-Amino-5-imidazole carboxamide, tris(trimethylsily 73
327 5000 237 17.20 17.40 17.60 17.80 45 m/z 147.00 12.40% 147 1 172 212 । $5 1 rq-rr | | " I j l i M | " 11" 'I' " i" " I''" i" " i"' ■ r'" i' i" "r' ■' i" " i m/z-> 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380400420 Abundance #56714: 1.1,1,5.7.7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73 — —.............. — 147 17,20 17.40 17,60 17.80 5000 267 m/z 324.90 8.85% 355 429 45 207 ! I TT m/z—> 40 60 80 100 120140160180200 220 240 260 280 300 320 340 360 380 400 420 Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 17.20 17.40 17.60 17.80 m/z 342.00 8.67% 5000 45 91 i 116 146 227 269 ‘‘I"TTTITTTTT PTUT ' i" " i ‘' "i" " i" " i' 1...... TT „[n ’1’1 I’315 r., m/z-> 40 60 80 100120 140160180 200 220 240 260 280 300 320340 360 380 400 420 17.20 17.40 17.60 17.80
29667.D GCMS1126.M Wed Jan 16 14:48:02 2002 Page 6
NYC-WTC_000036827
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NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018248
Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018123
Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder