Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
NYC-WTC_000019130–000019152Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 4-Amino-5-imidazole carboxamid Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.45 7.29 ug/1 2455090 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 32 2 1,1,1,5,7., /7,7-Heptamethyl-3 , 3-bis (t 444 C13H40O5Si6 038147-00-1 27 3 2H-1,4-B zodiazepin-2-one, 7-chlor 342 C18H19C1N2OSi 055299-24-6 12 4 Cyclohex siloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 10 Abundance t Scan 1351 (17.449 min): 30256.D (-) m/z 73.0,0 100.00% 73
5000 341 147
miz-> mkTgmanp 45 96 117 1. 179 207225 251 281 40 60 80 100120140160180200220240260280300320340360380400420 311 L t 397 429 t TTpTTrpTTTp-rtTp- 17.20 17.40 17.60 17.80 m/z 341.00 27.46% Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 % 327 5000 237 17.20 17.40 17*60 17.80 45 m/z 147.00 13.60%
miz-> 147 172 212 4s. *2d“80"‘20 100 'l20 ‘l40 *160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #56714 1,1.1.5.7.7.7-Heptamethy-3.3-bis(trimethylsiloxy)t 73
147 17.20 17.40 17.60 17.80 5000 267 m/z 325.00 9.57% 355 429 45 207
—uon)nu—BumOmu9n1—,Dm _ I _______________ TTIUDBuuuonuum —13DB3I0I......... ...... , ——CI—3WOUOB—BOBT"I7T1" m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340360380400420 Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 17.20 17.40 17.60 17.80 m/z 342.00 9.06% 5000 45 91 I 116 146 227 269 315 li TWTHTmmPTTTTTPTUTTTTmPWTTNTTTT ’ ’t’-’1’+*+**1’44’11 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30256.D GCMS1126.M Wed Jan 02 10:24:26 2002 Page 4 NYC-WTC_000019140
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NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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