NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 24 pages
GCMS analysis log for sample AD30712, Jan 2002
Machine-extracted title · confidence 100%Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
NYC-WTC_000018214–000018237Folder label: “GCMS X 12/27/01 A 1/16/02”
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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30712.D Vial: 35 Acq On 1 Jan 2002 9:53 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.45 8.28 ug/1 2137680 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7^iffeptamethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 35 2 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 17 3 2H-1,4-B znzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 12 4 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1351 (17.450 min): 30712.D (-) m/z 73.0,0 100.00% 73
5000 341 147 1 ' ‘ ' I ‘ ‘ ‘ ‘ I ' • 1 ‘ I ‘ ‘ ‘ ‘ I ' ‘ ‘ 45 , 17.20 17.40 17.60 17.80 i i t 97 117 | 041' “ i * “ TmmeaugmnemaggBm 179.. 207225 251 281 311 L h 397 429 m/z 341.00 27.15% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1.1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylslloxy)t 73
147 5000 267 355 429 17.20 17.40 17.60 17.80 45 207 m/z 147.00 13.60%
m/z-> kkmmM Tmgmoom pogp 40 60 80 100120140160180200220240260280300320340360380400420 Abundance 448317: 4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 -- 327 17.20 17.40 17.60 17.80 5000 m/z 325.00 9.21% 237 45 147 .255 | . 172 212 TTTTp-rrTp-rrTp-rrrp-rTTpr^ Tmmp m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 1*1** 1 . -j-i r'i ■ । । । i 73 341 17.20 17.40 17.60 17.80 m/z 342.00 9.00% 5000 45 91 | 116 146 227 269 315/ TpTmpmmmmpmpmmmpm] ________ ) V_________ ’AH8*11I444IIIV m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30712.D GCMS1126.M Wed Jan 23 08:42:45 2002 Page 5
NYC-WTC_000018225
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NYC-WTC_000036656
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