GCMS analysis log for sample AD30712, Jan 2002

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Data File C:\HPCHEM\1\DATA\DEC3101\30712.D Vial: 35 Acq On 1 Jan 2002 9:53 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS7 5K. L ********************************************************************* Peak Number 6 Acetamide, N-methyl- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

18.16 0.55 ug/1 154639 Acenaphthene-dl 0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetamide, N-methyl- 73 C3H7NO 000079-16-3 9 2 2-Butanol, 2 nitroso-, acetate (est 145 C6H11NO3 013880-90-5 9 3 3-Hexanethiol, 3-ethyl- 146 C8H18S 055956-00-8 9 4 2-Cyclopenten-1-one, 3-amino-2-meth ill C6H9NO 069687-85-0 9 Abundance / Scan 1428 (18.157 min): 30712.D (-) "m/z 43.00 100.00% 1 43 57 73 5000 111 95 ‘I kind 1 1 T 17.80 18.00 18,20 18.40 m/z-> 10 -364 —+ 20 30 40 50 60 70 85 1 1 I ’* ■ i ■ 80 90 —Pr 127 136 145 ■ I ■ • , । i 111 i'f i । 11 100 110 120 130 140 150 m/ z Abundance #287: Acetamide, N-methyl- 43 73 30 5000 58 TTI1 17.80 18.00 18.20 18.40 15 m/z 73.00 50.23% •' i ■ ■' ■ ii • • • ■ — I • ' ‘ ' I ‘ 1 ■ ' I 1 ' ‘ ' t' “ ' i' ' ‘ 1 1 , 1 1 11 1 'T'»»। i»• •' 11 • miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #8595 2-Butanol. 2-ntroso- acetate (ester! i 43 PTfREPmmfr 17.80 18.00 18.20 18.40 5000 m/z 111.10 38.71% 73

_2734 56 86 115 145 m/z-> * * I ‘ • • * I ’ ‘ 10 20 ’ I ’ ‘ ‘ ‘ I * 30 40 • • । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ • ■ ■ । ■' ■ ■ । 50 60 70 80 90 100 110 120 130 140 150 । ।1-11 1′44′1′44414444114

Abundance #8888: 3-Hexanethiol, 3-ethyl- 57 17.80 18.00 18.20 18.40 m/ z 24.28% 5000 75 97 112 .................. . .......... ,47 | 89 II 146 ‘ ‘ I ‘ * • *! ‘' ‘ ‘ I ’ * * • I ‘’ I ‘ ’1 1mmmp ■ ■ ''l < ■ ■ ‘I- 1 “ 11 ’ 11' • 1' 1111111111111 * i * • “ i ■ ■ ■ ■ i ' miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 17.80 18.00 18.20 18.40

30712.D GCMS1126.M Wed Jan 23 08:42:51 2002 Page 6

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