GCMS analysis results for sample AD30473, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC3101\30473.D Vial: 14 Acq On : 31 Dec 2001 11:37 pm Operator: 209 GALOS Sample : gems scan 12/14fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.14 ug/1 1093210 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 1,3-Dioxolane, Abundance 2-(3-bromo-5,5,5-tri352C10H16BrC1302 Scan 279 (7.609 min): 30473.D (-) 000000-00-0 9 m/ z 73.00 100.00% 73 5000 43 ........ —.... 87 103 7.20 7.40 7.60 7.80 8.00 38 | 50 55 50 67, । ' 1 I ' ' ' 1 1 1 1 1 1 I ' 1 1 1 I 111 1 r'-' ' > i ' ■ 1173 + 1 1 1 1 | । । । । । । m/z 43.00 33.34% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- : 73

5000 I 1 1 ‘ • I 1 11 14/55d*‘**I* 7.20 7.40 7.60 7.80 8.00 55 m/z .41.05 11.58% 45 87 27 39, ! • » I । » 1 i • • < • । > I* ... । . , । ■ • ) ■ I • ■ । । । । . vnfz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292; N-Ethylformamide 30 73 i ■ ' ' ' i ' 7.20 7.40 7.60 7.80 8.00 5000 m/ z 45.0, 11.33% 44 58 15 | miz-> 0 10 20 . j 30 । 40 ।।।।<i.,।* i * 50 60 70 80 90 । 100 110 , Abundance #763: 1-Butanamine, 3-methyl- । ,-n . yr. i I’I .it, । . l 11* 30 7.20 7.40 7.60 7.80 8.00 m/z 71.0.0 7.02% 5000

......... . 15 41 55 70 87 i ' ■ i ' - ' l ' ' ‘ ' I ' ' i ■ ' ■■■ i ' ■ i ■ ■ ■ ■ i ' ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30473.D GCMS1126.M Wed Jan 16 08:24:47 2002 Page 1

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