GCMS analysis results for sample AD30473, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC3101\30473.D Vial: 14 Acq On : 31 Dec 2001 11:37 pm Operator: 209 GALOS Sample : gems scan 12/14fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.68 14.21 ug/1 4941290 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 94 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 59 3 2H-l-Benzopyran-3-ol, 3,4-dihydro- 150 C9H10O2 021834-60-6 9 4 2-Cyclopenten-l-one, 2-(2-butenyl)- 150 C1OH140 017190-71-5 9 Abundance Scan 722 (11.676 min): 30473.D (-) m/z 150.00 100.00% 1:0

5000 115 52 78 11.40 11.60 11.80 12.00

m/z~> 30 38 44 , ’’I* TTTTft 63 -721TT 87 t t,. 99 108 ,| 122 132 1I"t . . >•)■> . ! > (•>■> 11111 • ■ i • • ■ ■ i • ■ r-ryrT m/z 151.90 63.51% 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593: 1,4-Dichlorobenzene-d4 150

.K 5000 115 - 1 ■ i • ■

52 78 11.40 11.60 11.80 12.00 m/z 115.00 39.61% 35 87 iT — ’ ।।■। । i ' ' m/z-> 30 • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । 40 50 60 70 80 90 I ‘ ‘ ‘ ‘ I • 100 110 120 130 140 150 160 Abundance #9592: Benzene-1.2.3.4-04-. 5.6-dichloro- 150

115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 27.27%

m/z-> Abundance

5000 30 35 ■ ‘ i' ' '11 ■1'' i 40 50 87 ■ ■ । ■■ ■ ■ ।■i ■ • ■• । ■ ■ * ■ । •• ■ ■ ।■11 ■11111 ■1111111 r1 1111‘1 60 70 80 90 100 110 120 130 #9708:2H-1-Benzopyran-3-ol, 3,4-dihydro- 107 140 150

150 160 1 1 • i ■ ■ 11.40 11.60 11.80 12.00 m/ Z 52.0.0 24.66%

78 119 131 miz-> ’I 1 1 * ‘ I 1 1 1 * I 1 * » * I 1 * * * { I I 30 40 50 60 70 189 i ■ ■ ■ ■ i ■ • ‘ ‘ i ■ ■ 80 90 Arl, 100 110 120 130 140 150 *14* 160 t I ‘ 1 TT-p-r 11.40 11.60 11,80 12.00

30473.D GCMS1126.M Wed Jan 16 08:24:52 2002 Page 2

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