GC/MS analysis results for sample AD30934, Jan 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30934.D Vial: 51 Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

7.61 4.52 ug/1 1107570 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 - Pentanol, 3 -methyl - 102 C6H140 000077-74-7 36 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1-But ammine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance • Scan 279 (7.608 min): 30934.D (-) m/z 72.95 100.00% 73

5000 43 1*‘*‘I*‘‘I‘I**I* “ I I I I

87 103 7.20 7.40 7.60 7.80 8.00 38 |, | 51 57. 67, । —IIIITIIN 1 . I . rrrp 1*I‘*‘I4" m/z 43.05 32.43% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 I ' ' ' ' I ' ‘ 1 ‘ I ' r 1 1 I TrT"I I I I 55 7.20 7.40 7.60 7.80 8.00 45 87 m/z 45.05 11.83% 27 1 Mr ■ 1 ■ 1 1 • i 1 1' • • I ■ • • 1 1 1 1 1 1 1 1 1 m/z-> Abundance 10 20 30 40 50 60 70 #292: N-Ethylformamide 80 90 100 110 30 73 7.20" 7.40 ' 7.60 7.80 8.00' 5000 m/z 41.00 11.49% 44 58 15 miz-> 10 20 +4 30 • । 40 50 * i ■ ■ ■ < i * • • * । ■ • • ■ । • ■ • ■ । ■ ■ ■ * । • ■ ■ < । 60 70 80 90 100 110 ।

Abundance #763: 1-Butanamine, 3-methyl- 2 TTI 1"! fT r | | | 1 IITTPrP 30 7.20 7.40 7.60 7.80 8.00 m/z 71.00 7.34% 5000

15 41 87 I 7 411 K ‘ i ‘ 55 1 i • • • ■ 70 I 1 ■ ‘ ‘ i ‘ • 1 ‘ i ‘ ‘ ' I 1 1 1 ' I 1 1 11 * * 61* » j । n I । i i m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30934.D GCMS1126.M Fri Jan 25 11:46:33 2002 Page 1

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