Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
NYC-WTC_000018733–000018753Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC3101\30934.D Vial: 51 Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS Sample gems scan 12 /19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
11.13 0.34 ug/1 83126 1,4 -Dichlorobenzene-d4 11.68
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 3,6-Bis (N-dimethylamino) -9-ethylcar 281 C18H23N3 057103-04-5 28 3 6,7-Benzo- phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 4- (1-Benzi midazyl)-7-nitro-2,1,3-ox 281 C13H7N5O3 091485-32-4 9 Abundance Scan 663 (11.134 min): 30934.D (-) m/z 281.00 100.00% 231
5000
miz-> Abundance 45 59 73 86 103 119 133 163 179 123 207 235 249 285 i r “trirt 1 P1t । ri i I । 'i i i i '| i' i #1 । r . . > I. ’1 . . T* । . . ) . . .! . . . . I . . . . I Ht 40 60 80 100 120 140 160 180 200 220 240 260 280 #41966: Cyclotetrasiloxane, octamethyl- m/z 7 Pp । । । । rap 10.80 11.00 11.20 11.40 ■ ■ i ■ • ■ • i
26.61%
201
5000 / 14/88* | 1 • f • ‘ | ‘ ‘ j 10.80 11.00 11.20 11.40 207 m/z 283.00 16.51% 73 133 1 163 177 191 - 235 249 265 | ■ ■ I ■ • i H • ■ • • । • ■ m/z-> ' 40 60 80 100 120 140 160 180 266 220 240 260 280 Abundance #39524; 3.6-Bis(N-dimethylamino)-9-ethylcarbazole 281 _________ ■ ■ I 1 ■ ■ ■ i ■ ■ • ■ i ' ■ ■ ' i 10.80 11.00 11.20 11.40 5000 m/z 192.90 12.14% 266
miz-> 1 40 ‘ do 141 80 100 120 140 160 180’ 200 220 240 260 280 208 222 23725 1 Abundance #39602:6,7-Benzo-phenothiazlne-5,5-dloxide » i । i i i I । » i V “i j i i i i । i i t > । 281 10.80 11.00 11.20 11.40 m/z 73.00 10.55% 5000 217 232 .................. 102 118 ............... 189 204. 1 252264 1 ■ ■ i ■ ' ■ ' i' • A • • i • • AM.M m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30934.D GCMS1126.M Fri Jan 25 11:46:37 2002 Page 2
NYC-WTC_000018741
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NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder