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Document / 27 pages

GCMS analysis results for sample AD29522, Jan 2002

Machine-extracted title · confidence 100%

Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.

NYC-WTC_000036752–000036778

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036758
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.0G MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclotetrasiloxane, octamethyl Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

11.13 3.64 ug/ 1949620 1,4-Dichlorobenzene-d4 11.68

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 80 2 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6, 7-Benzo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 4 3,6-BisKN-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 Abundance Scan 662 (11.126 min): 29522.D (-) m/z 281.0.0 100.00% 281

5000 ________ ■ • । • ■ ■ ■ । ■ ■ i ■ ■ ' ■ i ' ' 73 133 193

m/z-> 0- 45 59 | ■, v.. । y ... . । < 40 60 89 103 119 | 147 163 177 J 207 221 235 ■| . ”| T’T । . । T . . l"| . Tr ।-At 80 100 120 140 160 180 200 220 240 260 280 249 265 LL L m/z 282.00 10.80 11.00 11.20 11.40 28.54% Abundance #72646: Cyclotetrasiloxane, octamethyl- 1 281

5000 .................. / 10.80 11.00 11.20 11.40 265 m/z 283.00 18.01% 1 4559 .......... . 123297 . . ,235 miz--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrirni 281

10.80 11.00 11.20 11.40 5000 m/Z 192.90 12.53%

! 192 123 141 175 204 247 miz-2 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 281 10.80 11.00 11.20 11.40 m/ z 133.00 12.16% 5000-

217 232 102 118 189 204 44 1 ,, 252264 ■ । ■ ■ ■ । • ■ ' ' i ' ' ' ■ i fnlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

29522.D GCMS1126.M Fri Jan 18 16:48:07 2002 Page 1

NYC-WTC_000036758

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NYC-WTC_000036758Source: NYC Law Department, mirrored locally

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