NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC3101\29522.D Vial: 63
Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS
Sample gems scan 12/7 Inst : GC/MS 209
Mise Multiplr: 1.0G
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 1 Cyclotetrasiloxane, octamethyl Concentration Rank 20
R.T. EstConc Area Relative to ISTD R.T.
11.13 3.64 ug/ 1949620 1,4-Dichlorobenzene-d4 11.68
Hit# Of 5 entative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 80
2 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9
3 6, 7-Benzo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9
4 3,6-BisKN-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9
Abundance Scan 662 (11.126 min): 29522.D (-) m/z 281.0.0 100.00%
281
5000
________ ■ • । • ■ ■ ■ ।
■ ■ i ■ ■ ' ■ i ' '
73 133 193
m/z->
0-
45 59 |
■, v.. । y ... . । <
40 60
89 103 119 | 147 163 177 J 207 221 235
■| . ”| T’T । . । T . . l"| . Tr ।-At
80 100 120 140 160 180 200 220 240 260 280
249 265
LL L m/z 282.00
10.80 11.00 11.20 11.40
28.54%
Abundance #72646: Cyclotetrasiloxane, octamethyl-
1 281
5000 .................. /
10.80 11.00 11.20 11.40
265 m/z 283.00 18.01%
1 4559 .......... . 123297 . . ,235
miz--> 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrirni
281
10.80 11.00 11.20 11.40
5000 m/Z 192.90 12.53%
!
192 123 141 175 204 247
miz-2 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide
281 10.80 11.00 11.20 11.40
m/ z 133.00 12.16%
5000-
217 232
102 118 189 204 44 1 ,, 252264 ■ । ■ ■ ■ । • ■ ' ' i ' ' ' ■ i
fnlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
29522.D GCMS1126.M Fri Jan 18 16:48:07 2002 Page 1
NYC-WTC_000036758
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