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GCMS scan comments for sample AD30605

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

NYC-WTC_000017265–000017289

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017276
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17 Acq On : 9 Jan 2002 4:56 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P . Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Preeresererrrrrrrrrrterertere ffrrrrtrttrrrrrrtrtrtt ict t ttt ttt tte tres Peak Number 5 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 1 R.T. | EstCone Area Relative to ISTD R.T. 17.31 4.93 ug/)” 1520480 Naphthalene-d8 15.12 Hit# of 5 éntative ID MW MolForm cas# Qual 1 1,1,1,5,7/7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 25 2 2H-1,4-Bénzodiazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 12 3 Silane /[1,2,3-benzenetriyltris (oxy 342 C15H3003Si3 017864-23-2 12 4 4-Amiyo-5-imidazole carboxamide, tr_342 C13H30N40Si3__000000-00-0 9 (Abundance ‘Sean 1336 (17.306 min): 30605.D ) m/z 73.00 100.00 | i | 8000. | | 341 | 147 | | 48} 96 117 479, 207295 261 261 311 Pa any Te 5 ae ae miz->___” 40 6080 100 120 140 160 180 200 220 240 260 280 300 320 340 300 380 400.420 . . Abundance #56744: 1,1,1,5,7,7,7-Heplamethy/-3,3bls(trimethyisiiony}t t i | 147 | | | 267 355, 4og |-17.00_17.20_17.40__17.60 | 4s 207 | m/z 147.00 13.93 | \ fivz->____40_60_80_ 100.120 140 160 180 200220 240 260 280 300 320 340 360 380400420__ ‘Abundance. #48337; 2H-1 4-Benzodiazepin-2-ore, 7-chioro-1,3-dihydro-§- | 73 ant | | "woo Wviz0 1740 1760" | | 5000 m/z 325.00 9.923 | * ot | {i 116 146 27 200s s-> "0" 60 80 100 120 140 160 180:200 280 240 260 280 300 320 340 360 380 400 420, undance | #48324: Silane, [1,2,3-benzenetrlyitris(oxy)}tris[trimethyt- 47.00 17.20 _17.40_17.60 230 m/z 342.00 9.74 5000: 342 45 | 133479211 314 7 in 40 60 _80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400420 47.00 17.20 17.40. “17.60 ois 30605.D GCMS0103.M Tue Jan 15 09:31:15 2002 Page 5 NYC-WTC_000017276

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NYC-WTC_000017276Source: NYC Law Department, mirrored locally

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