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GCMS scan comments for sample AD30605

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

NYC-WTC_000017265–000017289

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017275
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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17 Acq On : 9 dan 2002 4:56 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc 3 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L. Perererrrrrrrrrrrerrerlrerrrrrrrrrrrert rrr te tirerrirrriri litre l irre rs Peak Number 4 Benzoic acid, 2,6-bis[(trimeth Concentration Rank 4 R.T. | EstConc Area Relative to ISTD R.T. 14.17 2.31 ug/l 713669 + Naphthalene-ds 15.12 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Benzoip’acid, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 40 2 Cyclogentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 39 3 BengOic acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 38 _4 N- (@rifluoroacetyl) -0,0',0''-tris(t 481 C19H34F3NO4Si3_000000-00-0 38 bundance, ® ‘Scan 984 (14.167 min): 30605.D ¢) m/z 73.00 100.00% i ] i} ] | 5000 | 267 385 | 45 493 254 13.80_14.00 14.20 14.40 | 89 108 133 154 177193 299 | 299 328390 We BeT 00 32618 miz—> ‘4060 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ‘Abundance "#51296: Benzdic acid, 2,6-bis[(trimethyisilyijoxyy, timet 3 | “| 000: 7 anal H 143.80 14.00 14.20 14.40 | | 147 267 m/z 355.0, 23.52% H 47 208 249 370 | Twz->__40_60_80_100 120 140 160 180 200 220 240 260 280 300 320 340 360 ‘Abundance #51286; Cyclopentasiloxane, Gecamethyl- | ii _ = (Rue WE — [m/z 268.00 8.78 i 191207 251 323339 > 40_60_80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ‘Roundance #73976: Benzoic acid, 2,5-bis(timethysiloxyy, trimethyis if 13.80 14.00 14.20 14.40 aR m/z 356.0, 8.75: | | 8000: | | 45 | weet! 179207223 267 370 | pz> "06'S" 150 TBO 140 180180 300 0S 260 360 SEN SHO 380.” | Galan” VaoO” “1490 “Wao 30605.D GCMS0103.M Tue Jan 15 09:31:11 2002 Page 4 NYC-WTC_000017275

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NYC-WTC_000017275Source: NYC Law Department, mirrored locally

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