GCMS analysis results for sample AD29667, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

■ Data File C:\HPCHEM\1\DATA\DEC3101\29667.D Vial: 56 Acq On 2 Jan 2002 8:14 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************************************************** * * * * * ** ** ** * * ***** Peak Number 8 Benzoic acid, 2,5-bis(trimethy Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

22.80 0.22 ug/1 114755 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 38 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 37 3 Benzenee anamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 Benzoic. acid, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 28 Abundance Scan 1934 (22.797 min): 29667.D (-) m/z 72.95 100.00% 73

5000 147 355 TTKnLmOT 11—— 221 281 401 22.40 22.60 22.80 23.00 23.20 r 1100— 1T150। । 1914 — —L , , 45 117 327 m/z-> —50 200 250 300 350 400 i

450 500 550 m/z 147.00 25.10% Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 355

5000 • । ' 22.40 22.60 22.80 23.00 23.20 45 m/z 355.05 24.37% J............ 147 179 223, 267,297 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 1 i • ■ ■ ■ i • - । 355 22.40 22.60 22.80 23.00 23.20 267 5000- m/z 221.05 18.00%

;...... ■ 207 .1 323 rn/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] \ i • ■ ■ ■ i > ■ • ■ i • ■ —1... 73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.00 14.86% 5000

45

m/z-> 11 50 100 150 208 251 281 IP-— 200 250 300 1 386 350 400 458 450 500 548 550 .. 4 TI""ELI1T 22.40 22.60 22.80 23.00 23.20

29667 .D GCMS1126.M Wed Jan 16 14:48:12 2002 Page 8

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