NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0302\29670.D Vial: 15
Acq On 4 Jan 2002 12 :13 am Operator: 209 GALOS
Sample gems scan 12/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT. P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 10 Benzoic acid, 2,5-bis(trimethy Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
22.64 0.27 ug/1 152636 Phenanthrene-dl0 24.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzoic acid, ,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 43
2 N- (Trifluorac etyl)-0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37
3 N- (Trifluoroacetyl) -0,0' ,0' ’-tris,(t 481 C19H34F3NO4Si3 000000-00-0 37
4. Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 32
Abundance Scan 1916 (22.637 min): 29670.D (-) m/ z 73.00 100.00%|
73
5000
147 355 -.... —
221 281 j
i 45 191 | 249 . j , 327 k 401 22.40 22.60 22.80 23.00
117
: —(+ PI 1 * L
m/ z 147.00 25.61%
m/z-> 50 100 150 200 250 300 350 400 450 500
Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls
I 73
355
5000-
22.40 22.60 22.80 23.00
45 m/ Z 355.05 23.22%
J....... .147 179 223 267 297... |_
m/z-> 50 100 150 200 250 300 350 400 450 500
Abundance #58807: N-(Trifluoracetyl)-O,O'.O"-tris(trirnetliylsilyl)epin
73
355 4
22.40 22.60 22.80 23.00
5000 m/z 221.05 16.85%
45
1. 140 184 281 | 480
■ ' i ' ■ ■ ■ i '
m/z-> 50 100 150 200 250 300 350 400 450 500
Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no A
I ‘ ' I ' '
73 22.40 22.60 22.80 23.00
355 m/ Z 281.00 14.17%
5000
45
| 1, 126147 193265 376 481
TB
miz-> 50 100 150 200 250 300 350 400 450 500 22.40 22.60 22.80 23.00
29670.D GCMS1126.M Wed Jan 16 14:51:11 2002 Page 10
NYC-WTC_000036858
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