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GCMS analysis results for sample AD29670, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036842–000036859

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036857
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\JAN0302\29670.D Vial: 15 Acq On 4 Jan 2002 12:13 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

20.86 0.21 ug/1 120079 Acenaphthene-diO 20.40

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 nisyl propionate 194 C11H1403 007549-33-9 47 3 Benzenepropanoic acid, 4-methoxy-, 194 C11H14O3 015823-04-8 43 4 Methylparaben 152 C8H803 000099-76-3 38 Abundance Scan 1722 (20.856 min): 29670.D (-) m/z 120.95 100.00% i 121

149 5000- 138 194 65 93 166 , 39

m/z-> 20 ........... - 30 4G 50,.4.76,..... L —1584 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 " i ■1'' i ■ " i" 20.60 20.80 21.00 21.20 m/z 149.00 49.92% Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 138 20.60 20.80 21.00 21.20 194 65 93 166 m/z 194.05 28.11% 27 I I , I ‘ ‘T | i' " ' i ,1..... 1 I " '' I' ’ * • I •' " I' " • I | > . 1 < ( I l ! * | < I ' . |

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21256: Anisyl propionate 121

20.60 20.80 21.00 21.20 5000 m/z 138.05 27.86% 77 91 194 138 I ' i" " i ■' T’TTTTT 111111111111 _. 199, i " '■i'■■>।।•■ ■ ■ ।■ I'''’I'’'’I“‘'I'‘"I I ■ r " ■ i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21262: Benzenepropanoic acid, 4-methoxy-, methyl ester / 121 20.60 20.80 21.00 21.20 m/ Z 65.05 17.71% 5000 - 194

LX 134 ‘i 108 i" " i" " i" " r ' " 11 ‘" I " " I "11111111111 'T 151 163 TTfTTTTI" ‘ * I ’' I4 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.60 20.80 21.00 21.20

29670.D GCMS1126.M Wed Jan 16 14:51:06 2002 Page 9

NYC-WTC_000036857

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NYC-WTC_000036857Source: NYC Law Department, mirrored locally

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