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GCMS analysis log for sample AD30605, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.

NYC-WTC_000018194–000018213

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018207
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30605.D Vial: 30 Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************* ******************************************************** Peak Number 7 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

21.09 0.41 ug/1 146982 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 'ethoxy-, ethyl este 194 C11H14O3 023676-09-7 96 2 Anisyl propio ate 194 C11H1403 007549-33-9 43 3 4-Methoxyphenylacetic acid ethyl es 194 C11H14O3 014062-18-1 43 4 Benzenepropanoic acid, 4-methoxy-, 194 C11H1403 015823-04-8 43 Abundance Scan 1748 (21.094 min): 30605.D (-) m/z 121.05 100.00% 121

5000 149 138 194 65 93 39 166 20.80 21.00 21.20 21.40 1 50 i,. 76 | 109 ■ 11■i.।.... ।।, TTITT m/z 149.00 45.01% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #69400: Benzoic acid, 4-ethoxy-, ethyl ester 121 149 5000 194 T T T T 138 20.80 21.00 21.20 21.40 65 93 166 m/z 194.05 28.80% .5°... .... 76.... | 50 1’11117 '■■I'1 "I”" I1 "‘111 “I11 ■ ■ i ■ ■ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21256; Anisyl propionate 121 -m Mpo , ■ 20.80 21.00 21.20 21.40 5000 m/z 138.05 28.75% ....... ................................. 77 91 194 138 109 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 '156' 160 170 180 190 200 Abundance #21247: 4-Methoxyphenylacetic acid ethyl ester 121 20.80 21.00 21.20 21.40 m/z 64.95 19.76% 5000 194

miz-> 51 65 ।।| I ...p.'. 1 ।.. .'I । 78 91 .'I'.| 106 | 148 I , ।('I।(।।. i i i 11 11 11 n i i | i l'i , 111 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 M.../Mo 20.80 21.00 21.20 2140 A

30605.D GCMS1126.M Wed Jan 23 08:29:00 2002 Page 7

NYC-WTC_000018207

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NYC-WTC_000018207Source: NYC Law Department, mirrored locally

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