GC/MS analysis results for sample AD30933, Jan 28 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30933.D vial: 50 Acq On 2 Jan 2002 2:22 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Benzoic acid, 2,5-bis(trimethy Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.80 0.77 ug/1 234453 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 35 2 N-(Trifluoracetyl) -0,0',0”-tris(tri 495 C20H36F3NO4Si3 000000-00-0 35 3 Benzeneetha: mine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 4 Trisiloxane , 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 Abundance Scan 1934 (22.797 min): 30933.D (-) m/z 73.00 100.00% 73

5000 147 355 221 281 22.40 22.60 22.80 23.00 23.20 , 45 117 191, | 249. [ 327 401 i 4 1 *'• 1 ' TmTTTemT i 450 500 m/z 147.00 2 6.88% miz-> 50 100 150 200 250 300 350 ' 400 550 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 355

5000 22.40 22.60 22.80 23.00 23.20 45 m/z 355.05 25.45% 147 179 223 267 297 1 i ■ ■ ■ • i■• ■ • ■ i • ■ • • i ■ • • ■ i • 1 ■ • I 1 ■ ■ ■ i ■ • • • 1 • ■ ' 1 1 ■ ■ ; • ■ i ' ‘ ' i • miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracety)-O,0’.0"tris(trimethylsilyl)epin 73 355 1*411104414418* 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 19.31%

45 140 184 281 480 * I • • TT9a—m)2—nBBm-0)mm—autm—uGmmur miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafiuorophenyI)methyIene] _ I I I [ > I t 1 , I I I I .

73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.00 15.84% 5000

45 208 251 281 386 458 548 • * । • * • • ।. • • • ।• TTNr ' 250 t+t l l < » ‘ I ‘ ‘ I I ‘ ‘ * I ‘ ‘ ‘ » I ‘ ‘ ‘ ‘l i > miz-> 50 100 150 200 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23'20

30933.D GCMS1126.M Fri Jan 25 11:43:36 2002 Page 6

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