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GCMS scan comments for sample AD30605

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

NYC-WTC_000017265–000017289

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”

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Scanned page image, NYC-WTC_000017274
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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17 Acq On : 9 Jan 2002 4:56 am Operator: 209 .GALOS Sample : gems scan 12/20 Inst. : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Prevrrrerrrrrrrrerertererrrrtrrrrrrrrttrrttrrttr itt tri t ttt ttt tt ttt rrr! Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 7 R.T. | EstCone Area Relative to ISTD R.T. 11.00 1.44 ug/l 354825 1,4-Dichlorobenzene-d4 11.52 Hit# of 5 tative ID MW MolForm CAS# Qual 1 Cyclotetrpgéiloxane, octamethyl- 296 C8H2404si4 000556-67-2 83 2 Benzene /1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50 3 2-Oxo-#-phenyl-6- (4-chlorophenyl) -1 282 C16H11C1N20 000000-00-0 9 _4 6,7-Bénzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 ‘Abundance ‘Scan 649 (10.968 min}: 30605.D () om | m/z 281.00 100.004 | | | os | cry 133 193 240 srry 207 285 40.60 10.80 "11.00 4120 11.40 H 45 59 gg 103 119 147 163. 221 235 m/z 282.10 27.583 jniz> 4060 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2 1 a! 40160 10.80 11.00 11.20 11.40 | m/z 283.00 17.77% i 3 183 agg 177 191 707 a9 249 265 hes 40 60 80 100 120 140 160 180 200 220 280 | ‘Abundance #00843; Benzene, 1-pheny!-4-(2-cyano-2-phenylethenyl) - | 1 | © ["yoleo"“tolso' “11100 “41120 “1140. | sooo | [m/z 192.90 12.82 { (253 1 126 203 224 240 266 fi iniz—> 4060 80 100 120 140 160 180 200 220 240 260 280 Abundance WES7EE: 2-Oxd-4-phony-8(6-chlorophery!)1,2-cihyaropyrint | 261 10.60_10.80 11.00 11.20 11.40 ; m/z 133.90 10.93% Hl 102 423 144 475-204 247 . ‘ancl 40 60. 80 1 120__ 4 160 '_ 180 220 240 260 260 10.60 10.80 11.00 11.20 11.40 30605.D GCMS0103.M Tue Jan 15 09:31:06 2002 Page 3 NYC-WTC_000017274

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NYC-WTC_000017274Source: NYC Law Department, mirrored locally

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