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GCMS analysis log for sample AD31076

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

NYC-WTC_000017514–000017528

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017522
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document a Library Search Compound Report * Data File : C:\HPCHEM\1\DATA\JAN0802\31076.D Vial: 9. i Acq On : 8 dan 2002 9:09 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE IIII ISIS SIS IIS ISHII SIO IIS IOI SEIIS ISH IG IO III III III II III Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 2 R.T. _ EstCone Area Relative to ISTD R.T. 11.00 1.90 ug/L 454777 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Cyclotetrasilgxane, octamethyl- 296 C8H2404Si4 000556-67-2 72 2 Benzene, 1-p¥fenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50 3 2-Oxo-4-pk€ényl-6- (4-chlorophenyl) -1 282 C16H11C1N20 000000-00-0 9 4 6,7-Ben&o-phenothiazine-5,5-dioxide 281 C16H11NO2S__000000-00-0 9 Abundancg “Scan 648 (10.995 min): 31076.5 -) ot m/z = 100. 00% 5000. j 73 ce 13 207 249 265 10.60_10.80_11.00_ 11.20 11.40 177 10.60 _10.80_11.00_11.20_11.40_ 45 59 89 103 149, 147 163 224 235 he q m/z 282.00 27.37: man 40 60.80 100 120 140 _160_180_200 220 240 280280. | | ‘Abundance #72646: Cyclotetrasiloxane, octamethy!- \ 1 40.60 10.60. 11:00 11.20 11.40 oe m/z 283.00 17.74 45 59 ds. 133 a77_198 207 235 h miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 ‘Abundance 7 40.60 10.80 11.00 11.20 11.40 5000 m/z 192-99 12.45) 253 126 0 | miz->.___40 6080100 _120 140 _160__180_200 220 240 280.260 | ‘Abundanes #39756: 2-Oxo-4-pheny-6-(4-chiorophenyi)-1,2-dinydropyrimi | 1 | 4060 “10.80 11.00 11.20 11.40, m/z 133,00 11.93 102423 141 175204 247 | | miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.60. 10.80 11.00 11.20 11.40 | 31076.D GCMS0103.M Wed Jan 09 12:30:10 2002 Page 2 NYC-WTC_000017522

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NYC-WTC_000017522Source: NYC Law Department, mirrored locally

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