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GCMS analysis log for sample AD31076

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

NYC-WTC_000017514–000017528

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017523
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NYC 9/11 Public Portal Document . i Library Search Compound Report . “Data File : C:\HPCHEM\1\DATA\JAN0802\31076.D Vial: 9 Acq On : 8 Jan 2002 9:09 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst. : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eereeerrrrrrr reser Sereeerrr reer rer rrr rrr rrr itt ttt tt ttt ttt ttt rrr ty Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. | EstCone Area Relative to ISTD R.T. 14.17 1.60 ug/l 471552 Naphthalene-d8 15.13 Hit# of 5 Tentative ID MW MolForm CASH Qual 1 Cyclopentas¥foxane, decamethyl- 370 C1OH3005Si5 000541-02-6 43 2 Benzoic agfd, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38 3 N-(TrifMioroacetyl) -0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 35 4.314-Dihydroxybenzyl alcohol, tris(tr_ 356 C16H3203Si3 __068595-79-9 35 Abundanes ‘Sean 994 (14.472 min}: 31076.0 (-) m/z y 100.00 258. 45 193 {13.80 _14.00_14.20_14.40_14.60 en 2a Se m/z 267.00 38.07 mz->___80__ 100 180 __200__250_300__350___ 400480. | ‘Abundances mi #51266: CyClopentasiloxane, decamethyl- | | | | 355 | 267 L \ aa | | {13.80 14.00 1420 44.40 wail | | H m/z 355.05 29.02 mz 50 100 150. 200 +250 = 300350 = 400-—S— 450 ‘Abundance | 73 13.80 14.00 14.20 14.40 14.60 5000. bl m/z 356.0; 10.078) 45 | 135193999 | mie> "60100" 150200250 900. 380. 400 ABD | ‘Abundance #58326: N-{Trifluoroacatyl)-O,0'0"-tis(trimethyisiiyiino | 13,80 14.00 14.20 14.40 14.60] ao m/z 268.00 9.728 a0 | | 45 | 126147193 265 376 481 | miz~> 50 100 150 200 250 300 350 400 450 13.80 14.00 14.20 14.40 “1460 31076.D GCMS0103.M Wed Jan 09 12:30:14 2002 Page 3 NYC-WTC_000017523

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NYC-WTC_000017523Source: NYC Law Department, mirrored locally

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GCMS analysis log for sample AD31073 · Box DEP Box 16

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

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GCMS analysis log for sample AD31024 · Box DEP Box 16

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

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GCMS scan comments for sample AD31017 · Box DEP Box 16

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Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

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GCMS scan comments for sample AD30605 · Box DEP Box 16

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Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

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