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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017444
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NYC 9/11 Public Portal Document 8 Library Search Compound Report “, + ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L FEISS ISI ISIS IIIS ISCO IOUT G IIE IIEI ISIE IST IOI IOEI IIIT III IIE Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstCone Area Relative to ISTD R.T. 14.16 4.92 ug/l 1523860 Naphthalene-d8 15.12 Hit# of 5 Tentative” ID MW MolForm CAS# Qual 1 Cyclopentasiloxgzfé, decamethyl- 370 C1OH3005Si5 000541-02-6 50 2 3,4-Dihydroxybénzyl alcohol, tris(tr 356 C16H3203Si3 068595-79-9 46 3 Benzoic acig/ 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 40 4 _N-(Trifluoyvoacety1) -0,0',O''-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 ‘Rbundancs ‘Scan 095 (14.164 mink 31073. () “| ave 73.00 | | 5000. i\ | 267 \ | 45 493 251 13.80_14,00_14.20_ 14.40 ___ 0. 89. a8. 133. 154. 17, 223 293 223590. m/z 267.0; 30.25) mniz->___40_60_80_100 120 140 160.180 200 220 240 260 280 300 320 340 360. ‘Abundance ' *#51266: Cyclopentasiloxané, decamethyi- | | \ 355 | | 287 , | | isleosaloo™“salz0" faa | lm/z 355.0 21.58% 191207 251 323339 | | miz->____40_60_ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 __ | ‘Abundance Headey 3.6 Uaydreere i 73 : / 131801400 14.20 14.40 5000. 179 aid [m/z 74.00 8.253% 386 | 45 147 209 237 | 312341 | miz-> ___40 60.80 100,120. 140 160 180 200 220 240 260 260 300 320 340 360. | \ | ‘Abundance #51206: Benzoic acid, 2,6-bis|(trimethyisily)jaxy)-, trimat 1 ; 3 1920 14.00 14.20 14.40 m/z 268.00 8.13 5000. | 167 287 47 208, 49 3 370 imiz—> 4060 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 1440 31073.D GCMS0103.M Wed Jan 09 12:19:06 2002 Page 3 NYC-WTC_000017444

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NYC-WTC_000017444Source: NYC Law Department, mirrored locally

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