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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017469
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document 5 . Library Search Compound Report “* Data File : C:\HPCHEM\1\DATA\JAN0802\31020.D Vial: 15 : Acq On : 9 Jan 2002 2:59 am Operator: 209 GALOS Sample : goms scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESU I SESS ISSO SSIS IOS SO IIIS JOTI OI IIIS IGE IOI IOI III Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstCone Area Relative to ISTD R.T. 14.17 3.09 ug/1 902944 Naphthalene-ds 15.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 CLOH3005Si5 000541-02-6 50 2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 40 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 38 ,4.3.4-Dihydroxybenzyl alcohol, tris (tr 356 C16H32038i3___068595-79-9 38 ‘Abundance ‘Scan 664 (74.168 min): 31020. () m/z 73.00 100.008 | = oe 267 355 \ | ol # 89 108 193 154 17193296223 251 | 293 328339 wees aa miz->___40_60__80_ 100 120140 160 180 200 220 240 260 280 300 320 340 360 _ “h . aa " #61266: Cyclopentasiloxane, decamethyi- | | x ] 365 | | som} | | | 13.80 1400 1420 1440 | | | | m/z 355.05 23.12 mz->___ 4060 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 _ | ‘Abundanice | ry 355 13.80 14.00 14.20 1440 __| 5000: | m/z 356.0 8.528 tar 267 | Lar 20g 249283 370 Deemer rrrepe rpererprery prep epee op rp Ee i | mz->___40 6080. 100 120 140 160 180 200 220 240 260 280 300 320 340 360_ | ‘Abundance #73978: Benzolc add, 2,5-bis(trimethyislloxyy., timethyis | 13.80_14.00 14.20 14.40 4 35 m/z 268.00 8.35% 5000. | 45 | 147479207223 267282207 370 | miz-> 49 60.80. 100 120 140 160 180 200 220 240 260 280 300 320 340 360 4900 1400 1420 1440. | 31020.D GCMS0103.M Wed Jan 09 12:11:37 2002 Page 4 NYC-WTC_000017469

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NYC-WTC_000017469Source: NYC Law Department, mirrored locally

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