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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report ‘+ Data File : C:\HPCHEM\1\DATA\JAN0802\31020.D Vial: 15 : Acq On : 9 Jan 2002 2:59 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JE SEIS IS ISIS SISO IOI IG SIE TORII HOISTS IOI ISIS IS IOUT TO ISI SOI II TO AE Peak Number 5 Cyclohexasiloxane, dodecamethy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.31 4.11 ug/l 1199690 Naphthalene-d8 15.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 38 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 25 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 22 _4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 __000000-00-0 17 ‘Abundance ‘Sean 1836 (17.306 min}: 31020.D G) j m/z 73.00 100.008) | 3a I | Ar —eeeperrecrd | 45 207. 429 17.00 17.20 17.40 17.60 96.117 179, 207295 261 21311 g01399 m/z 341-00 28.48% rmvz->_____40_60_80, 100 120 140 160 160200 220 240 260 260 300 320 340 360 380400420 | 344 | | | —sar alr 5000+ | a} ; 4 — | 47.00 1720 17:40_17.60 447 m/z 147.00 14.57% vz» "40" 60” 80.100 120 140 160 160 200 220 240 260 280 300 820 340 360 380 400420 I | Abundance rey 447 17.00 17.20 17.40 17.60 15000: 267 m/z 325.00 9.74% a5 429 : | miz-->__ 40_ 60.80 100.120 140 160 180 200 220 240 280 280 300 $20 340 360 380400420 | | Abundance #48337: 2H-1,4-Bonzodiazepin-2-one, 7-chloro-1,3-dihydro-5- | 7 Yi 17.00 1720 17.40 17.60 | m/z 342.00 9.29) 145 | | a | 17 nor 2 mo gi | rmiz-> "40 60. 80.100 120 140 160 180 200 220 240 260 260 300 320 340 360 380 400 420. | 17.00 17.20 17.40. 17.60 31020.D GCMS0103.M Wed Jan 09 12:11:41 2002 Page 5 NYC-WTC_000017470

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