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GCMS blank analysis results

Machine-extracted title · confidence 95%

Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

NYC-WTC_000017344–000017363

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document tee Library Search Compound Report _ /''* Data File : C:\HPCHEM\1\DATA\JANO802\LB.D vial: 7 Acq On : 8 Jan 2002 7:12 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc 3 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L. PeVreterrrrrrrrrer tert rerrrrrrrr tert tltrtttertrrt rire r rr rer rrr r res Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 1 R.T. EstConce Area Relative to ISTD R.T. 17.31 4.53 ug/l 1857460 § Naphthalene-ds 15.12 Hit# of 5 Tentative MW MolForm cAS# Qual 1 Cyclohexasiloxane,“dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 25 3 2H-1,4-Benzodgv4zepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 12 4 Silane, [1,7/3-benzenetriyltris (oxy 342 C15H3003Si3___017864-23-2 10 ‘Roundancs yy $08 1886,17.300 min LBD) [m/z 73.00 100.008 i 5000: | | oat | 147 45 . 207. 42g, 17.00 17.20 17.40 17.60 ‘s 99117 179, 207295 251 261311 397 herr | AE 341. 0p 29-318 mmvz>___” 40. 60. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 340 380 400.420 1 Abundance #56711: Cyclohexasiloxane, dodecamethyl- | % 34t | | 17.00 17.20 17.40. 17.60 | | | 147 | m/z 147.00 14.40 ee ee oe miz-> "40 60. 80 100 120 140 160 180 200 220 240 260 260 300 320 340 360 380 400420 | Abundance 73 | 447 17.00 17.20 17.40 17.60 5000+ 267 m/z 342.00 9.77 | 355 429 \ | L* 207 miz.-> 40. 60. 80 100 120 140 160 180.200 220 240 260 280 300 320 340 360 360 400 420 Abundance #48337; 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- o 17.00 17.20 17.40, 17.60 | m/z 325.0, 9.618 5000 | | 45 P| on | 146146 zr 269 ats . imiz-> "80" 60. 80 100 120 140 180 180 200 220 240 260 280 300 320 340 360 380 400 420 “700 1720 1740 1760 || LB.D GCMS0103.M Wed Jan 09 12:33:24 2002 Page 3 NYC-WTC_000017352

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NYC-WTC_000017352Source: NYC Law Department, mirrored locally

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