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GCMS blank analysis results

Machine-extracted title · confidence 95%

Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

NYC-WTC_000017344–000017363

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017351
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NYC 9/11 Public Portal Document ow Library Search Compound Report _ 7" Data File ; C:\HPCHEM\1\DATA\JAN0802\LB.D Vial: 7 Acq On : 8 Jan 2002 7:12 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS IS ISI ISIS ISIE IS ISIE ISIE ISIC IS ISGIS EIS ISHS SISSIES SSroiiaioiiiioi Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 5 R.T. EstCone Area Relative to ISTD R.T. 14.17 1.82 ug/l 745913 Naphthalene-ds 15.12 Hit# of 5 Tentative ID MW MolForm caAs# Qual 1 Cyclopentasiloxane/ decamethyl- 370 C10H3005Si5 000541-02-6 64 2 3,4-Dihydroxybe! 1 alcohol,tris(tr 356 C16H3203Si3 068595-79-9 46 3 Benzoic acid, 2/5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 38 _4 N-(Trifluorogéetyl) -0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 ‘Rourdance ‘Scan 004 (14.167 min} LB.D () m/z 73.00 100.008 i “ a ae 267 355 - 45 493 25 Taree aa | pik ee ponan tebe) m/z 267.00 32.60% ance ‘Hilts Sabpoiceloana toa | | 355 | 287 Pa | 13.80 14.00 14.20 14.40 “| m/z 355.0) 23.19% 191207 ast | a | miz-> "40 60. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360. | | Abundance | | 13 | | | 13.80 14.00 1420 1440." | 5000 479 eit m/z 356.05 8.37 356 i 5 147 } 209 _237 3t2__ 341 miz->____40_60_ 80_ 100 120 140 160 180 200 220 280 280 300 320 340 360 Abundance #73978: Benzoic acid, 2.5-bis(iimethyislioxyy, timethyls brent 43160 14,00. 14,20. 1440 355 m/z 268.00 8.30% 1 45 | 147479 207223 | 26790 370 I miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 9180 14.00 14.20 14.40 LB.D GCMS0103.M Wed Jan 09 12:33:19 2002 Page 2 NYC-WTC_000017351

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NYC-WTC_000017351Source: NYC Law Department, mirrored locally

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