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GCMS scan comments for sample AD31017

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

NYC-WTC_000017364–000017379

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017372
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document Library Search Compound Report * . + ‘Data File : C:\HPCHEM\1\DATA\JANO802\31017.D Vial: 13 Acq On : 9 dan 2002 1:02 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eeTeerrrrrrrrrerer rr rer rrrrrrrrretrtrr rit rrttt ttt rrr ttt iti tt ttt retry Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstCone Area Relative to ISTD R.T. 14.17 2.25 ug/l 733489 + Naphthalene-ds 15.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasivéxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Benzoic acj4, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 47 3 Benzoic g¢id, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 43 4_3,4-Dihydroxybenzyl alcohol, tris(tr 356 C16H3203Si3_ _068595-79-9 38 ‘Abundance ‘Scan 864 (14.166 min): 31017.D () “| m/z 73.00 100.008 | | 267 355 : - 45 193; 251 13.80_14.00 14.20 14.40 = 103118133 La uch 18223 293 S830, 4 in/z 267.00 33.44% miz>___40_60_80_100 120 140 160 180 200 220 240 260 280 300 320 340 360__| I | Abundance 3 *#51286: Cyélopentasiioxane, decamethyi- | | | | i | | 355 | | — 267 : i \ - 13.80 14.00 14.20 1440 m/z 355.0; 23.43: 191207, 251 323339 mlz» “40 60. 60.100 120 140 160 180 200 220 240 260 280 300 320 340 360 | ‘Abundance 73 355 13180 14.00 14.20 1440 000. m/z 268.00 9.20% 147 287 j \ | ae 20g 249283 370 rvz> 406080 100 120 140 100 180 200 220 240 260 280 300 320 340 300. | Abundance #73978: Benzoic acid, 2,5-bis(trimethyislioxy)-, trimethyls 13.80 14.00 14.20 1440 35 m/z 356.05 8.69) | : | | 147 479 297223 287 282207 370 mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 1440 31017.D GCMS0103.M Wed Jan 09 12:03:37 2002 Page 3 NYC-WTC_000017372 ‘

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NYC-WTC_000017372Source: NYC Law Department, mirrored locally

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