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GCMS scan comments for sample AD31017

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

NYC-WTC_000017364–000017379

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017373
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NYC 9/11 Public Portal Document Library Search Compound Report * . 3 “pata File : C:\HPCHEM\1\DATA\JAN0802\31017.D Vial: 13 Acq On : 9 dan 2002 1:02 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE ISI IESE ISIS HEI IO GI ITO GISI TOS SEI IOC IIE ISESISOTI ISG II III IOI Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2 R.T. | EstCone Area Relative to ISTD R.T. 17.31 3.07 ug/l 999615 = Naphthalene-d8 15.12 Hit# of 5 Tentative ID MW Mol Form cas# Qual 1 1,1,1,5,7,7,7-Keptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 27 2 2H-1,4-Benzo@lazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 22 3 3-Trimethy¥6ilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 17 4_CyclonexaSiloxane, dodecamethyl-___444 C12H3606Si6 ___000540-97-6 10 Rbundance ‘Sean 1396 (17.306 min}: 31017. @) os m/z 73.00 100.00 000 | 341 bie ave 207295 251 261 311 aor 429 47.00 17.20 17.40 17.60 ‘ i m/z 341.00 29.07 miz—>___40_60_80 100120 140 160 180 200 220 240 260 280 300 320 340 360380400420 \ Abundance. 7 ‘#56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(timethyisiloxy)t | | 147 000 | aif 355 429. |___17100 "17/20 “1740. 17.60 | | 207 | , ) [m/z 147.00 13.95 rmiz->__" 40. 60 80100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 | ‘Abundance i zee o 73 3a il 17.00 17.20 17.40_ 17.60 i Bond m/z 342.00 10.02 7 j a miz-->___40 60__80_100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400420 __ | Abundance #56734: 3-Trimethylsilyloxystearic acid, trimethyisilyl est Te | 17.00_17.20_17.40_17.60_ m/z 325.00 9.98 5000 147 233 | | 313 429 | miz-> "4060 80 100 120 140 160 180 200 220 240 280 280 300 320 340 360 380 400 420 1700 1720 1740 1760 || 31017.D GCMS0103.M Wed Jan 09 12:03:42 2002 Page 4 ' NYC-WTC_000017373

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NYC-WTC_000017373Source: NYC Law Department, mirrored locally

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