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GCMS blank analysis results

Machine-extracted title · confidence 95%

Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

NYC-WTC_000017344–000017363

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017357
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NYC 9/11 Public Portal Document ts Library Search Compound Report “+ pata File : C:\HPCHEM\1\DATA\JAN0802\LB.D Vial: 7 Acq On : 8 Jan 2002 7:12 pm Operator: 209 GALOS Saniple : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE SFI ISIS I IOI IOI ICIS I IO TIO TI ITI TTI TTT IT I Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8 R.T, | EstCone Area Relative to ISTD R.T. 26.73 0.85 ug/l 366510 Phenanthrene-d10 24.81 Hit# of 5 Tentatjve ID MW MolForm cas# Qual 1 3-Isopropoxy-1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 50 2 1-Monolinoles¥lglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 3 Ethanedioig’acid, bis(trimethylsily 234 CeHiso4si2 018294-04-7 32 _4 Trisiloxpfe, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 Rbandance ‘Scan 2363 (26.736 min): LB.D C) 7 m/z 73.00 100.00% | 147 | } 224 281 + | 355 26.40 26.60 26.80 27.00 0. 45 147, 7 191 249, 327, 7 401 429 m/z 147.00 32 04 mizn>___50___100___150__200___250._ 300 __350___400__450__500 __§50_ | “Abundance * #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim “= | Co oe as ae | m/z 281.00 16. 654 22° 281 | miz-> 50 100. 150 200 250 300 350. 400 450 500 550 | ‘Abundancs | 7 | or 2640 26.60 26160 2700" 5000! 147 m/z 221.0, 15.11 m. 103 | 281 ; 395 482 | mz-> 80.100 150200 __250_300__350__400__450__500__ 580 _ } Boo Aa etaodo 6, lees) Slr = i} 167 ___ 28.40 26.60 26.80_27.00 m/z 74.00 8.49) 45 | 190 249 miz-> 50 100 150 200 250 300 350 400 460 500 550 | 2640 26.60 26.80 27.00 LB.D GCMS0103.M Wed Jan 09 12:33:46 2002 Page 8 NYC-WTC_000017357

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NYC-WTC_000017357Source: NYC Law Department, mirrored locally

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